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By De Sombre, Harvey, Nagabhushanam, Ohashi, Peterson & Rauhut) T. Howard Austin et al (Berlin

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N. Haszeldine, J. Chem. , 1963, 1083. 24. Burg, A. , and A. P. Caron, J. Am. Chern. , 81, 836 (1959). 25. Burg, A. , and P. J. , J. Am. Chern. , 80, 1107 (1958). 26. , and N. D. Dawson, J. Org. , 16, 1250 (1951). 27. Cadogan, J. 1. , Quart. , 16, 208 (1962). 28. Campbell, 1. G. , and J. K. Way, Proc. Chem. , 1959, 231. 29. Campbell, 1. G. , and J. K. Way, J. Chern. , 1960, 5034. 30. Campbell, 1. G. , and J. K. -Chem. , 1961,2133. 31. , and J. F. Wilkinson, J. Chem. , 1924,2675. 32. Christen, P.

And G. B. Butler, J. Org. , 25,2006 (1960). 13. Berlin, K. , and G. B. Butler, J. Am. Chem. , 82, 2712 (1960). 14. Berlin, K. , and G. B. Butler, J. Org. , 26,2537 (1961). 15. Berlin, K. , and M. Nagabhushanam, in press. 16. Berlin, K. , and M. Peterson, unpublished results. 17. Blount, B. , J. Chem. , 1931, 1891. 18. Blount, B. , J. Chem. , 1932, 337. 19. Braye, E. , and W. Hubel, Chem. Ind. (London), 1959, 1250. 20. Browning, M. , J. R. Mellor, D. J. Morgan, S. A. J. Pratt, L. E. Sutton, and L.

With a large excess of phosphoryl chloride, phosphonic dichlorides, phosphinic chlorides, and o O~PCI3 R = catalyst + t RMgX -------+ RPCI 2 CH 3 , C 2H s ; catalyst = pyridine 0 + t R 2PCI + R3P~O phosphine oxides were isolated (96). The yields were below 20% for all products in these examples,. Complexes bet,veen magnesium salts and the acid halides were broken only by heating in vacuo at 150-300° (96). The discrepancy between this data and that cited previously (114,157) should be resolved by additional experimentation.

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