By De Sombre, Harvey, Nagabhushanam, Ohashi, Peterson & Rauhut) T. Howard Austin et al (Berlin
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With a large excess of phosphoryl chloride, phosphonic dichlorides, phosphinic chlorides, and o O~PCI3 R = catalyst + t RMgX -------+ RPCI 2 CH 3 , C 2H s ; catalyst = pyridine 0 + t R 2PCI + R3P~O phosphine oxides were isolated (96). The yields were below 20% for all products in these examples,. Complexes bet,veen magnesium salts and the acid halides were broken only by heating in vacuo at 150-300° (96). The discrepancy between this data and that cited previously (114,157) should be resolved by additional experimentation.